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Beamline 11.3.1 Print
Tuesday, 20 October 2009 09:22

 

Small-molecule crystallography

Beamline 11.3.1 web site

Scientific disciplines: Structural chemistry, magnetic materials, microporous materials.

 

GENERAL BEAMLINE INFORMATION

Operational

Yes

Source characteristics

Bend magnet

Energy range

6–17 keV

Monochromator

Channel-cut Si(111)

Flux (1.9 GeV, 400 mA)

1x1011 photons/s/0.01%BW at 10 keV

Resolving power (E/ΔE)

1000

Endstations

Medium sized hutch with Bruker AXS D8 diffractometer and Oxford Cryosystems Cryostream Plus

Detectors

Bruker AXS APEXII CCD

Spot size at sample

280 µm x 90 µm (100-µm diameter with collimator)

Samples

 

Sample format

Crystals as small as 15 µm x 15 µm x 15 µm

Sample preparation

Mount in oil in a mitegen loop

Sample environment

90–500 K nitrogen open flow system

Special notes

Bruker AXS APEX2 software for data collection and processing. SHELXTL software suite for structure solution and refinement.

Experimental techniques

Single crystal x-ray diffraction

Scientific applications

Chemical crystallography

Scientific disciplines Structural chemistry, magnetic materials, microporous materials.

Local contact / Spokesperson

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Advanced Light Source, Berkeley Lab
Phone: (510) 486-4457
Fax: (510) 486-7696

Beamline phone number

(510) 495-2117