|
Small-molecule crystallography
Scientific disciplines: Structural chemistry, magnetic materials, microporous materials.
| GENERAL BEAMLINE INFORMATION |
|
Operational
|
Yes
|
|
Source characteristics
|
Bend magnet
|
|
Energy range
|
6–17 keV
|
|
Monochromator
|
Channel-cut Si(111)
|
|
Flux (1.9 GeV, 400 mA)
|
1x1011 photons/s/0.01%BW at 10 keV
|
|
Resolving power (E/ΔE)
|
1000
|
|
Endstations
|
Medium sized hutch with Bruker AXS D8 diffractometer and Oxford Cryosystems Cryostream Plus
|
|
Detectors
|
Bruker AXS APEXII CCD
|
|
Spot size at sample
|
280 µm x 90 µm (100-µm diameter with collimator)
|
|
Samples
|
|
|
Sample format
|
Crystals as small as 15 µm x 15 µm x 15 µm
|
|
Sample preparation
|
Mount in oil in a mitegen loop
|
|
Sample environment
|
90–500 K nitrogen open flow system
|
|
Special notes
|
Bruker AXS APEX2 software for data collection and processing. SHELXTL software suite for structure solution and refinement.
|
|
Experimental techniques
|
Single crystal x-ray diffraction
|
|
Scientific applications
|
Chemical crystallography
|
| Scientific disciplines |
Structural chemistry, magnetic materials, microporous materials. |
|
Local contact / Spokesperson
|
This e-mail address is being protected from spambots. You need JavaScript enabled to view it
Advanced Light Source, Berkeley Lab Phone: (510) 486-4457 Fax: (510) 486-7696
|
|
Beamline phone number
|
(510) 495-2117
|
|